These visuals are made from the original lecture transparencies
- Gradient pulse leads to twisted coherence
- Gradient-Enhanced HSQC: 3 gradient pulses
- General Setup Procedure for DRX-500
- Setting Up the 2D Spectral Window
- The 2D Spectral Window: Bruker Parameters
- Number of Data Points in 2D Experiment
- 2D NMR Parameters: Bruker
- Menu Display after eda Command (Page 1)
- Menu Display after eda Command (Page 2)
- Data Processing in Two Dimensions
- Window Functions for 2D NMR: Bruker Parameters
- Phase Errors in Two Dimensions
- Interactive 2D Phase Correction
- Menu Display after edp Command
- Cholesterol 1H and 13C Spectra Arranged on x and y Axes
- Cholesterol 1H and 13C Spectra with Two HSQC Crosspeaks
- Expansion of Downfield Region: Cholesterol HSQC with 1D Spectra
- Cholesterol HSQC Spectrum with 1H and 13C Spectra
- Cholesterol HSQC Spectrum
- Expansion of Upfield Region: Cholesterol HSQC with 1D Spectra
- Edited 13C-Decoupled HSQC of Cholesterol
- F2 slices at carbons j, q and s of Cholesterol HSQC
- HSQC / HMQC and HMBC
- One-bond vs 2-3 bond correlations
- 13C-decoupled HSQC of sucrose in D2O (500 MHz, gradients)
- HMBC of sucrose in D2O
- HMBC of sucrose in D2O, with overlay of HSQC spectrum
- HMBC of sucrose in D2O, with diagram of 2 and 3 bond correlations
- HMBC of sucrose in D2O: upfield region
- HSQC Spectrum of Product 2: Expanded Region
- 1D 1H Spectrum of Product 2: Two expansions (overlay)
- HMBC Spectrum of Product 2: Expanded Region (overlay)
- Conformational Effects in HMBC
- 2D-COSY (Correlation Spectroscopy)
- COSY and DQF-COSY
- Homonuclear Shift Correlation: COSY
- 3-heptanone in CDCl3: DQF-COSY Spectrum 600 MHz
- 3-heptanone: DQF-COSY with H1-H2 Spin System
- 3-heptanone: DQF-COSY with H4-H5-H6-H7 Spin System
- 3-heptanone: DQF-COSY with Assignments and Correlation Diagram
- 3-heptanone: DQF-COSY showing artifacts
- DQF-COSY Spectrum of Sucrose (Full Matrix)
- 300 MHz COSY Spectrum of Sucrose: Full Spectrum
- DQF-COSY Spectrum of Sucrose: H(g1) - H(g2) Crosspeak Fine Structure
- 300 MHz COSY Spectrum of Sucrose: Upfield Region
- 600 MHz COSY Spectrum of Sucrose: Upfield Region
- Double-Quantum Filtered COSY
- Coherence pathway selection using gradients
- 2D-TOCSY
- TOCSY overview
- 3-heptanone in CDCl3: Simulated TOCSY Spectrum
- 3-heptanone in CDCl3: TOCSY Spectrum 72 ms mixing 600 MHz
- 3-heptanone in CDCl3: Overlay for TOCSY Spectrum
- TOCSY of Heregulin-alpha
- 2D-NOESY (Nuclear Overhauser Effect Spectroscopy)
- NOESY overview
- Gradient-Enhanced NOESY
- Measurement of crosspeak volumes (sucrose NOESY)
- NOESY Spectrum of Unknown F
- NOESY Correlations for Unknown F, 13C Spectrum of Unknown F
- 2D-ROESY (Rotating Frame Overhauser Effect Spectroscopy)
- Maximum Theoretical Overhauser Effect
- The Spin-Lock
- ROESY Pulse Sequence Diagram
- ROESY of Pristimerin Oxidation Product, olefinic to upfield
- ROESY of Pristimerin Oxidation Product, olefinic to upfield, with Structure Diagram
- Pristimerin Oxidation Product Structure with Distances and 1H Spectrum